1 Aperçu de la méthode
After sample pretreatment, lead ions form a complex with sodium diethyldithiocarbamate (DDTC) under a specific pH condition. The complex is extracted and separated using 4-methyl-2-pentanone (MIBK), then introduced into an atomic absorption spectrometer for flame atomization. Absorbance is measured at a wavelength of 283.3 nm. Within a certain concentration range, the absorbance of lead is proportional to its mass content, and quantification is performed by comparison with a standard series.
2. Champ d'application
This method applies to the determination of lead in sodium pyrophosphate food additive.
3 Reference Standards
GB 25557-2010 National Food Safety Standard – Food Additive Sodium Pyrophosphate, Section A.10 Determination of Lead
4 Instruments, Equipment and Reagents
4.1 Instruments et équipements
4.1.1 Analytical Instruments
表格
| - Non, non. | Nom | Quantité | Exigences techniques | Accessoires |
| 1 | Spectrophotomètre d'absorption atomique de flamme | 1 ensemble | — | Lampe cathodique creuse au plomb |
| 2 | Compresseur d'air | 1 unité | Pression nominale d'échappement: 0,3 MPa | — |
| 3 | Acetylene Cylinder | 1 cylindre | Pureté ≥ 99,99% | — |
