1 نظرة عامة على الطريقة
After sample pretreatment, lead ions form a complex with sodium diethyldithiocarbamate (DDTC) under a specific pH condition. The complex is extracted and separated using 4-methyl-2-pentanone (MIBK), then introduced into an atomic absorption spectrometer for flame atomization. Absorbance is measured at a wavelength of 283.3 nm. Within a certain concentration range, the absorbance of lead is proportional to its mass content, and quantification is performed by comparison with a standard series.
2 نطاق التطبيق
This method applies to the determination of lead in sodium pyrophosphate food additive.
3 Reference Standards
GB 25557-2010 National Food Safety Standard – Food Additive Sodium Pyrophosphate, Section A.10 Determination of Lead
4 Instruments, Equipment and Reagents
4.1 الأدوات والمعدات
4.1.1 Analytical Instruments
表格
| -لا | اسم | كمية | المتطلبات التقنية | مُكَمِّلات |
| 1 | مقياس الطيف للامتصاص الذري للهب | 1 مجموعة | — | مصباح الكاثود الرصاص المجوف |
| 2 | ضاغط الهواء | وحدة واحدة | ضغط العادم المسمى: 0.3 ميجا باس | — |
| 3 | Acetylene Cylinder | أسطوانة واحدة | النقاء ≥ 99.99٪ | — |