1 نظرة عامة على الطريقة
The sample is digested with hydrochloric acid, hydrogen peroxide and nitric acid solution. In dilute hydrochloric acid medium, the absorbance of iron is measured by air‑acetylene flame at the wavelength of 248.3 nm using an atomic absorption spectrometer.
2 نطاق التطبيق
This method is applicable for the determination of iron in zinc alloys.
3. المعيار المرجعي
GB/T 12689.5‑2004 Chemical analysis methods for zinc and zinc alloys — Determination of iron content — Sulfosalicylic acid spectrophotometry and flame atomic absorption spectrometry, Method 2: Flame atomic absorption spectrometry
4 Apparatus and Reagents
4.1 Apparatus and Equipment
4.1.1 Testing Instruments
| -لا | اسم | كمية | المتطلبات التقنية | مُكَمِّلات |
|---|---|---|---|---|
| 1 | مقياس الطيف للامتصاص الذري للهب | 1 مجموعة | — | Iron hollow‑cathode lamp |
| 2 | ضاغط الهواء | 1 مجموعة | Rated discharge pressure: 0.3 MPa | — |
| 3 | الأسيتيلين | أسطوانة واحدة | Purity ≥99.99% | — |