1 Methodenblick
The sample is heated and dissolved in a quartz beaker with mixed sulfuric phosphoric acid. Using an air acetylene flame, the absorbance of sodium oxide is measured at 589.0 nm on an atomic absorption spectrophotometer. Within a certain concentration range, the absorbance of sodium is proportional to its content, and quantification is carried out by comparison with the standard series.
2 Anwendungsbereich
This method is applicable to the determination of sodium oxide content in alumina powder.
3 Reference Basis
GB/T 6609.5-2004, Methods for chemical analysis and physical property testing of alumina — Determination of sodium oxide content, Method 2
4 Instrumente und Reagenzien
4.1 Instrumente und Ausrüstung
4.1.1 Testing Instruments
| - Nein. - Nein. | Name | Menge | Technische Anforderung | Zubehör |
| 1 | Atomic Absorption Spectrophotometer (TAS 990) | 1 Satz | — | Sodium Hollow-Cathode Lamp |
| 2 | Luftkompressor | 1 Satz | Nenndruck: 0,3 MPa | — |
| 3 | Acetylen | 1 Zylinder | Purity ≥99.99% | — |
