GC-MS<\/u><\/a>\u00a0k\u1ebft h\u1ee3p hai c\u00f4ng c\u1ee5 m\u1ea1nh m\u1ebd: quang ph\u1ed5 kh\u00ed (GC) v\u00e0 quang ph\u1ed5 kh\u1ed1i l\u01b0\u1ee3ng (MS). H\u00e3y ngh\u0129 v\u1ec1 GC nh\u01b0 m\u1ed9t h\u1ed9p ph\u00e2n lo\u1ea1i. N\u00f3 chia h\u1ed7n h\u1ee3p c\u00e1c h\u1ee3p ch\u1ea5t d\u1ef1a tr\u00ean c\u00e1ch d\u1ec5 d\u00e0ng ch\u00fang bi\u1ebfn th\u00e0nh kh\u00ed v\u00e0 d\u00ednh v\u00e0o m\u1ed9t v\u1eadt li\u1ec7u \u0111\u1eb7c bi\u1ec7t trong m\u1ed9t c\u1ed9t. Sau \u0111\u00f3, MS h\u00e0nh \u0111\u1ed9ng nh\u01b0 m\u1ed9t th\u00e1m t\u1eed. N\u00f3 t\u00ecm ra m\u1ed7i h\u1ee3p ch\u1ea5t l\u00e0 g\u00ec b\u1eb1ng c\u00e1ch ki\u1ec3m tra t\u1ef7 l\u1ec7 kh\u1ed1i l\u01b0\u1ee3ng-s\u1ea1c c\u1ee7a n\u00f3. C\u00f9ng nhau, ch\u00fang l\u00e0 m\u1ed9t c\u1eb7p ho\u00e0n h\u1ea3o \u0111\u1ec3 ph\u00e2n t\u00edch nh\u1eefng th\u1ee9 d\u1ec5 bay h\u01a1i, ch\u1eb3ng h\u1ea1n nh\u01b0 nh\u1eefng th\u1ee9 trong thu\u1ed1c, m\u1eabu m\u00f4i tr\u01b0\u1eddng ho\u1eb7c ki\u1ec3m tra an to\u00e0n th\u1ef1c ph\u1ea9m.<\/p>\n\u0110\u00e2y l\u00e0 c\u00e1ch n\u00f3 \u0111i: b\u1ea1n l\u1ea5y m\u1ed9t m\u1eabu v\u00e0 l\u00e0m n\u00f3ng n\u00f3 cho \u0111\u1ebfn khi n\u00f3 l\u00e0 m\u1ed9t kh\u00ed. Sau \u0111\u00f3, b\u1ea1n g\u1eedi n\u00f3 qua m\u1ed9t c\u1ed9t GC. C\u00e1c h\u1ee3p ch\u1ea5t \u0111\u01b0\u1ee3c t\u00e1ch ra d\u1ef1a tr\u00ean c\u00e1c \u0111\u1eb7c \u0111i\u1ec3m \u0111\u1ed9c \u0111\u00e1o c\u1ee7a ch\u00fang. Ti\u1ebfp theo, ch\u00fang ch\u1ea3y v\u00e0o quang ph\u1ed5 kh\u1ed1i l\u01b0\u1ee3ng. N\u00f3 l\u00e0m ch\u00fang th\u00e0nh ion v\u00e0 t\u1ea1o ra m\u1ed9t m\u00f4 h\u00ecnh \u0111\u1eb7c bi\u1ec7t - nh\u01b0 d\u1ea5u v\u00e2n tay - cho m\u1ed7i m\u1ed9t. \u0110i\u1ec1u n\u00e0y gi\u00fap b\u1ea1n x\u00e1c \u0111\u1ecbnh v\u00e0 \u0111o l\u01b0\u1eddng c\u00e1c h\u1ee3p ch\u1ea5t v\u1edbi \u0111\u1ed9 ch\u00ednh x\u00e1c tuy\u1ec7t v\u1eddi. N\u1ebfu b\u1ea1n c\u1ea7n c\u00e1c c\u00f4ng c\u1ee5 \u0111\u00e1ng tin c\u1eady, G5 GC c\u1ee7a ch\u00fang t\u00f4i \u0111\u01b0\u1ee3c x\u00e2y d\u1ef1ng \u0111\u1ec3 x\u1eed l\u00fd t\u1ea5t c\u1ea3 c\u00e1c lo\u1ea1i c\u00f4ng vi\u1ec7c t\u00e1ch d\u1ec5 d\u00e0ng.<\/p>\n
<\/p>\n
L\u1ee3i th\u1ebf v\u00e0 h\u1ea1n ch\u1ebf c\u1ee7a quang ph\u1ed5 kh\u00ed v\u00e0 quang ph\u1ed5 kh\u1ed1i l\u01b0\u1ee3ng<\/h2>\n
GC-MS l\u00e0 m\u1ed9t v\u1ea5n \u0111\u1ec1 l\u1edbn trong c\u00f4ng vi\u1ec7c ph\u00f2ng th\u00ed nghi\u1ec7m, nh\u01b0ng n\u00f3 kh\u00f4ng ho\u00e0n h\u1ea3o. H\u00e3y xem n\u00f3 l\u00e0m g\u00ec t\u1ed1t v\u00e0 n\u00f3 c\u00f3 th\u1ec3 g\u1eb7p b\u1ea1n \u1edf \u0111\u00e2u. B\u1eb1ng c\u00e1ch n\u00e0y, b\u1ea1n c\u00f3 th\u1ec3 quy\u1ebft \u0111\u1ecbnh xem n\u00f3 c\u00f3 ph\u00f9 h\u1ee3p v\u1edbi nhu c\u1ea7u c\u1ee7a b\u1ea1n kh\u00f4ng.<\/p>\n
S\u1ee9c m\u1ea1nh c\u1ee7a c\u00e1c k\u1ef9 thu\u1eadt<\/h3>\n\u0110\u1ed9 nh\u1ea1y c\u1ea3m v\u00e0 \u0111\u1ed9 \u0111\u1eb7c bi\u1ec7t cao<\/h4>\n
GC-MS c\u00f3 th\u1ec3 t\u00ecm th\u1ea5y m\u1ed9t l\u01b0\u1ee3ng v\u1eadt ch\u1ea5t si\u00eau nh\u1ecf - xu\u1ed1ng \u0111\u1ebfn ph\u1ea7n tr\u00ean t\u1ef7 (ppb) ho\u1eb7c th\u1eadm ch\u00ed ph\u1ea7n tr\u00ean ngh\u00ecn t\u1ef7 (ppt). H\u00e3y t\u01b0\u1edfng t\u01b0\u1ee3ng th\u1ea5y m\u1ed9t gi\u1ecdt n\u01b0\u1edbc \u00e9p trong m\u1ed9t h\u1ed3 b\u01a1i l\u1edbn. \u0110\u00f3 l\u00e0 lo\u1ea1i s\u1eafc n\u00e9t m\u00e0 ch\u00fang ta \u0111ang n\u00f3i v\u1ec1. \u0110i\u1ec1u n\u00e0y l\u00e0m cho n\u00f3 tuy\u1ec7t v\u1eddi cho c\u00e1c nhi\u1ec7m v\u1ee5 nh\u01b0 ki\u1ec3m tra thu\u1ed1c tr\u1eeb s\u00e2u trong th\u1ef1c ph\u1ea9m ho\u1eb7c ch\u1ea5t \u00f4 nhi\u1ec5m trong n\u01b0\u1edbc. Th\u00eam v\u00e0o \u0111\u00f3, MS l\u00e0 tuy\u1ec7t v\u1eddi trong vi\u1ec7c x\u00e1c \u0111\u1ecbnh ch\u00ednh x\u00e1c c\u00e1c h\u1ee3p ch\u1ea5t. V\u00ec v\u1eady, b\u1ea1n s\u1ebd kh\u00f4ng b\u1ecb nh\u1ea7m l\u1eabn b\u1edfi nh\u1eefng th\u1ee9 t\u01b0\u01a1ng t\u1ef1 trong c\u00e1c m\u1eabu kh\u00f3 kh\u0103n.<\/p>\n
S\u1ef1 linh ho\u1ea1t trong ph\u00e2n t\u00edch c\u00e1c m\u1eabu ph\u1ee9c t\u1ea1p<\/h4>\n
GC-MS gi\u1ed1ng nh\u01b0 m\u1ed9t c\u00f4ng c\u1ee5 \u0111a d\u1ea1ng. N\u00f3 ho\u1ea1t \u0111\u1ed9ng v\u1edbi t\u1ea5t c\u1ea3 c\u00e1c lo\u1ea1i m\u1eabu, t\u1eeb kh\u00f4ng kh\u00ed \u0111\u1ebfn m\u00e1u. Cho d\u00f9 b\u1ea1n \u0111ang ki\u1ec3m tra c\u00e1c manh m\u1ed1i hi\u1ec7n tr\u01b0\u1eddng t\u1ed9i ph\u1ea1m ho\u1eb7c nghi\u00ean c\u1ee9u d\u1ea7u, n\u00f3 c\u00f3 th\u1ec3 x\u1eed l\u00fd c\u00e1c h\u1ed7n h\u1ee3p kh\u00f3 kh\u0103n. M7 GC-MS c\u1ee7a ch\u00fang t\u00f4i l\u00e0m cho \u0111i\u1ec1u n\u00e0y th\u1eadm ch\u00ed \u0111\u01a1n gi\u1ea3n h\u01a1n v\u1edbi c\u00e1c c\u00e0i \u0111\u1eb7t b\u1ea1n c\u00f3 th\u1ec3 \u0111i\u1ec1u ch\u1ec9nh \u0111\u1ec3 ph\u00e2n t\u00edch c\u00e1c m\u1eabu kh\u00e1c nhau nhanh ch\u00f3ng v\u00e0 ch\u00ednh x\u00e1c.<\/p>\n
Th\u00e1ch th\u1ee9c v\u00e0 h\u1ea1n ch\u1ebf<\/h3>\nT\u00e1c \u0111\u1ed9ng v\u1ec1 chi ph\u00ed<\/h4>\n
Thi\u1ebft l\u1eadp GC-MS chi ph\u00ed r\u1ea5t nhi\u1ec1u. Thi\u1ebft b\u1ecb r\u1ea5t \u0111\u1eaft. B\u1ea1n c\u0169ng c\u1ea7n ph\u1ea3i tr\u1ea3 ti\u1ec1n b\u1ea3o tr\u00ec, ch\u1eb3ng h\u1ea1n nh\u01b0 kh\u00ed tinh khi\u1ebft cao ho\u1eb7c c\u1ed9t. \u0110\u00f3 l\u00e0 m\u1ed9t chi ph\u00ed l\u1edbn ban \u0111\u1ea7u. Nh\u01b0ng k\u1ebft qu\u1ea3 l\u00e0 \u1ed5n \u0111\u1ecbnh v\u00e0 \u0111\u00e1ng tin c\u1eady, c\u00f3 th\u1ec3 l\u00e0m cho n\u00f3 \u0111\u00e1ng gi\u00e1. Ph\u00f2ng th\u00ed nghi\u1ec7m c\u1ee7a b\u1ea1n n\u00ean suy ngh\u0129 v\u1ec1 vi\u1ec7c li\u1ec7u chi ph\u00ed c\u00f3 ph\u00f9 h\u1ee3p v\u1edbi m\u1ee5c ti\u00eau v\u00e0 ng\u00e2n s\u00e1ch c\u1ee7a b\u1ea1n hay kh\u00f4ng.<\/p>\n
Y\u00eau c\u1ea7u chuy\u00ean m\u00f4n k\u1ef9 thu\u1eadt<\/h4>\n
Ch\u1ea1y GC-MS kh\u00f4ng gi\u1ed1ng nh\u01b0 nh\u1ea5n n\u00fat. B\u1ea1n c\u1ea7n nh\u1eefng ng\u01b0\u1eddi bi\u1ebft c\u00e1ch thi\u1ebft l\u1eadp ph\u01b0\u01a1ng ph\u00e1p, \u0111i\u1ec1u ch\u1ec9nh m\u00e1y m\u00f3c v\u00e0 hi\u1ec3u d\u1eef li\u1ec7u. N\u1ebfu kh\u00f4ng t\u1eadp luy\u1ec7n, b\u1ea1n c\u00f3 th\u1ec3 kh\u00f4ng \u0111\u1ea1t \u0111\u01b0\u1ee3c k\u1ebft qu\u1ea3 t\u1ed1t nh\u1ea5t. \u0110\u00f3 l\u00e0 l\u00fd do t\u1ea1i sao ch\u00fang t\u00f4i t\u1ea1i PERSEE cung c\u1ea5p h\u1ed7 tr\u1ee3 th\u1ef1c t\u1ebf v\u00e0 \u0111\u00e0o t\u1ea1o \u0111\u1ec3 gi\u00fap \u0111\u1ed9i ng\u0169 c\u1ee7a b\u1ea1n s\u1eb5n s\u00e0ng s\u1eed d\u1ee5ng h\u1ec7 th\u1ed1ng c\u1ee7a ch\u00fang t\u00f4i.<\/p>\n