{"id":5208,"date":"2026-09-10T16:32:37","date_gmt":"2026-09-10T08:32:37","guid":{"rendered":"https:\/\/www.pgeneral.com\/?p=5208"},"modified":"2026-09-10T16:32:37","modified_gmt":"2026-09-10T08:32:37","slug":"determination-of-lead-in-olive-oil-graphite-furnace-atomic-absorption-spectrometry-4","status":"publish","type":"post","link":"https:\/\/www.pgeneral.com\/pt\/applications\/determination-of-lead-in-olive-oil-graphite-furnace-atomic-absorption-spectrometry-4","title":{"rendered":"Determina\u00e7\u00e3o do chumbo no \u00f3leo de oliva"},"content":{"rendered":"<p>1 Resumo do M\u00e9todo<br \/>\nAp\u00f3s a digest\u00e3o por micro-ondas, a solu\u00e7\u00e3o da amostra \u00e9 injetada no forno de grafite do espectrofot\u00f4metro de absor\u00e7\u00e3o at\u00f4mica. Ap\u00f3s a atomiza\u00e7\u00e3o eletrot\u00e9rmica, absorve a linha de resson\u00e2ncia em 283,3 nm. Dentro de uma determinada faixa de concentra\u00e7\u00e3o, o valor da absorb\u00e2ncia \u00e9 proporcional ao teor de chumbo, e a quantifica\u00e7\u00e3o \u00e9 realizada por compara\u00e7\u00e3o com uma s\u00e9rie de padr\u00f5es.<\/p>\n<p>2. \u00c2mbito de aplica\u00e7\u00e3o<br \/>\nEste m\u00e9todo \u00e9 aplic\u00e1vel \u00e0 determina\u00e7\u00e3o de chumbo no azeite.<\/p>\n<p>3 Base de Refer\u00eancia<br \/>\nGB 5009.12\u20112017<\/p>\n<p>4 Instrumentos e Reagentes<\/p>\n<p>4.1 Instrumentos e equipamento<\/p>\n<p>4.1.1 Instrumentos de teste<\/p>\n<table>\n<thead>\n<tr>\n<th>N\u00e3o.<\/th>\n<th>Nome<\/th>\n<th>Quantidade<\/th>\n<th>Requisitos t\u00e9cnicos<\/th>\n<th>Acess\u00f3rios<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>1<\/td>\n<td>Espetrofotometro de Absor\u00e7\u00e3o At\u00f4mica do Furno de Graf\u00edto<\/td>\n<td>1 conjunto<\/td>\n<td>\u2014<\/td>\n<td>L\u00e2mpada de c\u00e1todo oco de chumbo<\/td>\n<\/tr>\n<tr>\n<td>2<\/td>\n<td>Arg\u00f4nio<\/td>\n<td>1 cilindro<\/td>\n<td>Pureza \u226599,99%<\/td>\n<td>\u2014<\/td>\n<\/tr>\n<tr>\n<td>3<\/td>\n<td>Sistema de \u00e1gua refrigerante circulante<\/td>\n<td>1 conjunto<\/td>\n<td>\u2014<\/td>\n<td>\u2014<\/td>\n<\/tr>\n<\/tbody>\n<\/table>","protected":false},"excerpt":{"rendered":"<p>1 Method Overview After microwave digestion, the sample solution is injected into the graphite furnace of the atomic absorption spectrophotometer. After electrothermal atomization, it absorbs the resonance line at 283.3\u202fnm. Within a certain concentration range, the absorbance value is proportional to the lead content, and quantification is performed by comparison with the standard series. 2 [&hellip;]<\/p>\n","protected":false},"author":2,"featured_media":5209,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[36,73],"tags":[],"class_list":["post-5208","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-applications","category-food-and-drugs"],"acf":[],"_links":{"self":[{"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/posts\/5208","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/comments?post=5208"}],"version-history":[{"count":1,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/posts\/5208\/revisions"}],"predecessor-version":[{"id":5210,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/posts\/5208\/revisions\/5210"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/media\/5209"}],"wp:attachment":[{"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/media?parent=5208"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/categories?post=5208"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.pgeneral.com\/pt\/wp-json\/wp\/v2\/tags?post=5208"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}