\u539f\u7406
\n\u30d4\u30ea\u30c0\u30d9\u30f3\u6b8b\u57fa\u306f\u3001\u30b2\u30eb\u900f\u904e\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff08GPC\uff09\u307e\u305f\u306fSPE\u306b\u3088\u3063\u3066\u7cbe\u88fd\u3055\u308c\u3001GC-ECD\u304a\u3088\u3073GC-MS\u306b\u3088\u308b\u78ba\u8a8d\u306b\u3088\u3063\u3066\u6e2c\u5b9a\u3055\u308c\u305f\u3001\u30a2\u30bb\u30c6\u30fc\u30c8\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3\u307e\u305f\u306f\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\u3067\u62bd\u51fa\u3055\u308c\u307e\u3057\u305f\u3002<\/p>\n
\u8a66\u85ac\u3068\u6750\u6599
\n\u4f7f\u7528\u3055\u308c\u308b\u3059\u3079\u3066\u306e\u8a66\u85ac\u306f\u3001\u7279\u306b\u6307\u5b9a\u304c\u306a\u3044\u9650\u308a\u3001\u5206\u6790\u7684\u306b\u7d14\u7c8b\u3067\u306a\u3051\u308c\u3070\u306a\u308a\u307e\u305b\u3093\u3002
\n1\u3002\u9162\u9178\u30a8\u30c1\u30eb\uff1aHPLC\u30b0\u30ec\u30fc\u30c9\u3002
\n2\u3002\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3\uff1aHPLC\u30b0\u30ec\u30fc\u30c9\u3002
\n3\u3002\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb\uff1aHPLC\u30b0\u30ec\u30fc\u30c9
\n4\u3002\u30d8\u30ad\u30b5\u30f3\uff1aHPLC\u30b0\u30ec\u30fc\u30c9\u3002
\n5\u3002\u30c8\u30ea\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\uff1aHPLC\u30b0\u30ec\u30fc\u30c9\u3002
\n6\u3002\u7121\u6c34\u786b\u9178\u30ca\u30c8\u30ea\u30a6\u30e0;
\n4\u6642\u9593\u3001\u3057\u3063\u304b\u308a\u3068\u9589\u3058\u305f\u5bb9\u5668\u306b\u4fdd\u7ba1\u3057\u307e\u3059\u3002
\n7\u3002\u5869\u5316\u30ca\u30c8\u30ea\u30a6\u30e0\u3002
\n8\u3002\u9162\u9178\u30a8\u30c1\u30eb +\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3\uff081 + 1\u3001V\/V).
\n9\u3002\u30d8\u30ad\u30b5\u30f3 +\u30c8\u30ea\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\uff089 + 1\u3001V\/V).
\n10\u3002\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3 +\u9162\u9178\u30a8\u30c1\u30eb\uff086 + 1\u3001V\/V)
\n11\u3002\u30d4\u30ea\u30c0\u30d9\u30f3\u6a19\u6e96\uff08\u30d4\u30ea\u30c0\u30d9\u30f3\uff1aCAS No. 96489-71-3\uff1a\u5206\u5b50\u5f0fC19H25CIN2OS;\u5206\u5b50\u91cf\uff1a364\u300293;\u7d14\u7c8b\uff1a99\uff05\uff09\u3002
\n12\u3002\u6a19\u6e96\u7684\u306a\u30b9\u30c8\u30c3\u30af\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\uff1a\u4e00\u5b9a\u91cf\u306e\u30d4\u30ea\u30c0\u30d9\u30f3\u6a19\u6e96\u306e\u91cd\u91cf\u3092\u6b63\u78ba\u306b\u6bd4\u8f03\u691c\u8a0e\u3057\u3001\u5c11\u91cf\u306e\u9162\u9178\u30a8\u30c1\u30eb\u3067\u89e3\u304d\u307e\u3059\u3002
\n13.\u6a19\u6e96\u4f5c\u696d\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\uff1a\u6b21\u306b\u3001\u6a19\u6e96\u4f5c\u696d\u6eb6\u6db2\u3068\u3057\u3066\u3001\u9162\u9178\u30a8\u30c1\u30eb\u3067\u6a19\u6e96\u30b9\u30c8\u30c3\u30af\u6eb6\u6db2\u3092\u5fc5\u8981\u306a\u6fc3\u5ea6\u306b\u5e0c\u91c8\u3057\u307e\u3059\u3002
\n14\u3002\u30ab\u30fc\u30dc\u30f3-PSA-\u30c1\u30e5\u30fc\u30d6\uff1a1ml\u300150mg\u30013ML\u30a2\u30bb\u30c8\u30cb\u30c8\u30ea\u30eb +\u9162\u9178\u30a8\u30c1\u30eb\uff0810\uff09
\n15\u3002HLBSPE\u30c1\u30e5\u30fc\u30d6\uff1a3 mL\u300160 mg\u3001\u307e\u305f\u306f\u540c\u7b49\u3002
\n\uff089\uff09\u3001\u958b\u59cb\u524d\u306b2 mL\u306e\u30c8\u30ea\u30af\u30ed\u30ed\u30e1\u30bf\u30f3\u30685 mL\u306e\u84b8\u7559\u6c34\u3092\u3002
\n16\u3002\u30d5\u30a3\u30eb\u30e0\uff1a0.45\u03bcm\u3002<\/p>\n
\u88c5\u7f6e\u3068\u6a5f\u5668
\n1\u3002\u30ac\u30b9\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff1aECD\u3092\u88c5\u5099
\n2\u3002\u30ac\u30b9\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\uff1a\u96fb\u5b50\u30a4\u30aa\u30f3\u5316\u8cea\u91cf\u5206\u6790\u3092\u88c5\u5099\u3002
\n3\u3002\u5206\u6790\u30d0\u30e9\u30f3\u30b9\uff1a0.01 g\u306e\u611f\u899a\u3002
\n4\u3002\u5206\u6790\u30d0\u30e9\u30f3\u30b9\uff1a0.1 mg\u306e\u611f\u899a
\n5\u3002ISOCRATIC\u30dd\u30f3\u30d7\u3068\u5206\u6570\u30b3\u30ec\u30af\u30bf\u30fc\u3092\u88c5\u5099\u3057\u305f\u30b2\u30eb\u900f\u904e\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u3002
\n6.\u9060\u5fc3\u5206\u96e2\u6a5f\uff1a4000r\/min\u3002
\n7\u3002\u56de\u8ee2\u771f\u7a7a\u84b8\u767a\u5668
\n8\u3002\u7121\u6c34\u786b\u9178\u30ca\u30c8\u30ea\u30a6\u30e0\u30ab\u30e9\u30e0\uff1a7.5 cm x 1.5 cm\uff08i\u3002d\u3002\uff095 cm\u306e\u5438\u53ce\u6027\u7dbf\u306e\u71c3\u6599\u5145\u586b\u786b\u9178\u30ca\u30c8\u30ea\u30a6\u30e0\u3092\u6e80\u305f\u3057\u307e\u3057\u305f\u3002
\n9\u3002Vortex\u30df\u30ad\u30b5\u30fc\u3002
\n10\u3002\u8d85\u97f3\u6ce2\u30de\u30b7\u30f3\u3002
\n11\u3002\u30db\u30e2\u30b8\u30ca\u30a4\u30b6\u30fc\u3002
\n12\u300250ml\u505c\u6b62\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u9060\u5fc3\u5206\u96e2\u6a5f\u30c1\u30e5\u30fc\u30d6\u3002<\/p>\n
\u30c6\u30b9\u30c8\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099\u3068\u4fdd\u5b58
\n\u30c6\u30b9\u30c8\u30b5\u30f3\u30d7\u30eb\u306e\u6e96\u5099
\n1\u3002\u30b7\u30ea\u30a2\u30eb\u3068\u8336
\n\u30b5\u30f3\u30d7\u30eb\u3092CA\u306b\u56db\u5206\u306e\u4e00\u306b\u3002
\n2\u3002\u679c\u7269\u3068\u91ce\u83dc
\n\u7d50\u5408\u3055\u308c\u305f\u4e00\u6b21\u30b5\u30f3\u30d7\u30eb\u306fCA\u306b\u7e2e\u5c0f\u3055\u308c\u307e\u3059\u3002<\/p>\n
3\u3002\u8089\u3068\u8089\u88fd\u54c1\u3001\u30ca\u30c3\u30c4
\n\u4ee3\u8868\u8005\u3092\u7d041 kg\u306e\u30b5\u30f3\u30d7\u30eb\u306b\u3057\u307e\u3059\u3002<\/p>\n
\u30c6\u30b9\u30c8\u30b5\u30f3\u30d7\u30eb\u306e\u4fdd\u5b58
\n\u30b7\u30ea\u30a2\u30eb\u3001\u8336\u3001\u30ca\u30c3\u30c4\u3001\u9162\u3001\u8702\u871c\u3001\u8702\u871c\u306e\u88fd\u54c1\u306e\u30c6\u30b9\u30c8\u30b5\u30f3\u30d7\u30eb\u306f\u30010\u301c4\u00b0\u306e\u9593\u306b\u4fdd\u7ba1\u3059\u308b\u5fc5\u8981\u304c\u3042\u308a\u307e\u3059\u3002<\/p>\n
\u624b\u9806
\n\u62bd\u51fa
\n1\u3002\u91ce\u83dc\u3001\u679c\u7269\u3002
\n\u8a66\u9a13\u30b5\u30f3\u30d7\u30eb10g\uff08\u7cbe\u5ea60.01g\uff09\u309250mL\u306e\u30b9\u30c8\u30c3\u30d1\u30fc\u4ed8\u304d\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u88fd\u9060\u5fc3\u7ba1\u306b\u5165\u308c\u3001\u9162\u9178\u30a8\u30c1\u30eb+\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f320mL\u3092\u52a0\u3048\u30661000\/\u5206\u30671\u5206\u9593\u30db\u30e2\u30b8\u30ca\u30a4\u30ba\u62bd\u51fa\u3057\u305f\u5f8c\u30014000\/\u5206\u30673\u5206\u9593\u9060\u5fc3\u5206\u96e2\u3057\u3001\u4e0a\u6f84\u307f\u6db2\u3092\u5225\u306e\u6e05\u6f54\u306a\u7ba1\u306b\u79fb\u3057\u3001\u9162\u9178\u30a8\u30c1\u30eb+\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f320mL\u3067\u518d\u5ea6\u62bd\u51fa\u64cd\u4f5c\u3092\u7e70\u308a\u8fd4\u3057\u307e\u3059\u3002\u4e0a\u6f84\u307f\u6db2\u3092\u7121\u6c34\u786b\u9178\u30ca\u30c8\u30ea\u30a6\u30e0\u306e\u30ab\u30e9\u30e0\u306b\u901a\u3057\u3066\u6c34\u3092\u9664\u53bb\u3057\u3001\u6d41\u51fa\u6db2\u3092150mL\u6fc3\u7e2e\u74f6\u306b\u96c6\u3081\u300140\u2103\u306e\u30a6\u30a9\u30fc\u30bf\u30fc\u30d0\u30b9\u3092\u5099\u3048\u305f\u30ed\u30fc\u30bf\u30ea\u30fc\u30a8\u30d0\u30dd\u30ec\u30fc\u30bf\u30fc\u3067\u307b\u307c\u4e7e\u71e5\u3059\u308b\u307e\u3067\u6fc3\u7e2e\u3057\u307e\u3059\u3002\u6b8b\u7559\u7269\u3092\u9162\u9178\u30a8\u30c1\u30eb+\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f310.0mL\u3067\u6eb6\u89e3\u3057\u30010.45\u03bcm\u306e\u30e1\u30f3\u30d6\u30e9\u30f3\u30d5\u30a3\u30eb\u30bf\u30fc\u3067\u6ffe\u904e\u3057\u3066\u7cbe\u88fd\u3092\u5f85\u3061\u307e\u3059\u3002<\/p>\n
2\u3002\u30af\u30eb\u30df\u3002
\n\u30c6\u30b9\u30c8\u30b5\u30f3\u30d7\u30eb\u306e\u91cd\u91cf10\uff080.01 g\u306b\u6b63\u78ba\uff0950 mL\u306e\u505c\u6b62\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u9060\u5fc3\u6027\u30c1\u30e5\u30fc\u30d6\u306b\u3002<\/p>\n
3\u3002\u8336\u3068\u7389\u306d\u304e
\n\u91cd\u91cf2\u30025g\uff080.01 g\u306e\u7cbe\u5ea6\uff09\u306e\u30b5\u30f3\u30d7\u30eb\u300150 mL\u306e\u505c\u6b62\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u9060\u5fc3\u5206\u96e2\u6a5f\u30c1\u30e5\u30fc\u30d6\u306b\u300115 ml\u306e\u84b8\u7559\u6c34\u3092\u52a0\u3048\u30011\u6642\u9593\u8010\u3048\u307e\u3059\u3002
\n\u4e0a\u6e05\u3092\u7121\u6c34\u786b\u9178\u30ca\u30c8\u30ea\u30a6\u30e0\u306e\u67f1\u306b\u901a\u3057\u3001\u6c34\u3092\u9664\u53bb\u3057\u3001\u6392\u6c34\u3092150 mL\u306e\u6fc3\u7e2e\u30dc\u30c8\u30eb\u306b\u96c6\u3081\u300140\u00b0\u306e\u6c34\u200b\u200b\u6d74\u3092\u5099\u3048\u305f\u56de\u8ee2\u84b8\u767a\u5668\u306b\u3088\u3063\u3066\u307b\u307c\u4e7e\u71e5\u3059\u308b\u3088\u3046\u306b\u51dd\u7e2e\u3057\u307e\u3059\u3002<\/p>\n
\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7
\n\u91ce\u83dc\u306e\u679c\u7269\u3001\u7a40\u7269\u3001\u30af\u30eb\u30df\u3001\u9d8f\u306e\u809d\u81d3\u306e\u305f\u3081\u306eGPC\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u3002
\n1\u3002GPC\u52d5\u4f5c\u6761\u4ef6
\na\uff09GPC\u30ab\u30e9\u30e0\uff1a300 mm 10 mm\uff08i\u3002d\u3002\uff09\u3001\u30d0\u30a4\u30aa\u30d3\u30fc\u30baS-x3\u307e\u305f\u306f\u540c\u7b49\u7269\uff1a
\nb\uff09\u79fb\u52d5\u76f8\uff1a\u9162\u9178\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3 - \u30a8\u30c1\u30eb\uff081+1\uff09\uff1a
\nc\uff09\u6d41\u91cf\uff1a4\u30027ml\/min:
\nd\uff09\u30b5\u30f3\u30d7\u30eb\u30eb\u30fc\u30d7\u3067\u306e\u6ce8\u5165\u91cf\uff1a5 ml\uff1a
\ne\uff09\u6eb6\u51fa\u7269\u3092\u53ce\u96c6\u3059\u308b\u6642\u9593\uff1a7.5\u5206\u301c12\u3002<\/p>\n
2\u3002GPC\u30af\u30ea\u30fc\u30f3\u30a2\u30c3\u30d7\u30b9\u30c6\u30c3\u30d7<\/p>\n
\u6700\u521d\u306e\u30b9\u30c6\u30c3\u30d7\u306b\u793a\u3055\u308c\u3066\u3044\u308b\u30d1\u30e9\u30e1\u30fc\u30bf\u30fc\u3092\u4f7f\u7528\u3057\u3066\u3001\u524d\u306b\u53d6\u5f97\u3057\u305f\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\u3092GPC\u306e\u5217\u306b\u8ee2\u9001\u3057\u307e\u3059\u3002
\n\u6eb6\u51fa\u306f\u304d\u308c\u3044\u306a\u30c1\u30e5\u30fc\u30d6\u306b\u53ce\u96c6\u3055\u308c\u3001\u7a92\u7d20\u306e\u6d41\u308c\u306e\u4e0b\u306735\u2103\u3067\u4e7e\u71e5\u3057\u3066\u84b8\u767a\u3057\u3001\u6e2c\u5b9a\u3068\u7acb\u4f53\u5316\u306e\u305f\u3081\u306b1.0 mL\u306e\u9162\u9178\u30a8\u30c1\u30eb\u3067\u518d\u6eb6\u89e3\u3057\u307e\u3059\u3002<\/p>\n
3.\u9162\u3068\u8702\u871c\u306e\u305f\u3081\u306eSPE\u30af\u30ea\u30fc\u30cb\u30f3\u30b0\u30a2\u30c3\u30d7
\n\u91cd\u91cf2.5 g\u306e\u30b5\u30f3\u30d7\u30eb\u3092\u30d7\u30e9\u30b9\u30c1\u30c3\u30af\u9060\u5fc3\u5206\u96e2\u6a5f\u306b\u5165\u308c\u30015 mL\u306e\u84b8\u7559\u6c34\u3068\u6e26\u309230\u79d2\u9593\u52a0\u3048\u307e\u3059\u3002<\/p>\n
4\u3002\u304a\u8336\u3068\u30bf\u30de\u30cd\u30ae\u306e\u6383\u9664
\n\u524d\u306b\u7372\u5f97\u3057\u305f\u6eb6\u6db2\u3092\u70ad\u7d20PSA\u30c1\u30e5\u30fc\u30d6\u306b\u79fb\u3057\u30011.5 mL\u306e\u30b7\u30af\u30ed\u30d8\u30ad\u30b5\u30f3 +\u9162\u9178\u30a8\u30c1\u30eb\u3067\u3059\u3059\u304e\u307e\u3059\u3002<\/p>\n
GC\u6c7a\u5b9a
\nGC\u64cd\u4f5c\u6761\u4ef6
\na\uff09\u5217\uff1aDB-1301 30 M0\u300225mm\uff08I.D.\uff09x0\u300225UM\u307e\u305f\u306f\u540c\u7b49\u3002
\nb\uff09\u30ab\u30e9\u30e0\u6e29\u5ea6\uff1a50\u2103\uff0820\u00b0\/min\uff09 - 200\u2103\uff085\u00b0\/min\uff09 - 260\u2103\uff0810\u5206\uff09\u3002
\nc\uff09\u6ce8\u5165\u30dd\u30fc\u30c8\u6e29\u5ea6\uff1a260 C\uff1a
\nd\uff09ECD\u6e29\u5ea6\uff1a300 C\uff1a
\ne\uff09\u30ad\u30e3\u30ea\u30a2\u30ac\u30b9\uff1a\u7a92\u7d20\uff08\u7d14\u5ea6> 99.999\uff05\u6d41\u91cf\uff1a2 ml {{url_placeholder_0}}\uff09;
\nf\uff09\u5674\u5c04\u30e2\u30fc\u30c9\uff1a\u30b9\u30d7\u30ea\u30c3\u30c8\u30ec\u30b9\u3002
\nG\uff09\u6ce8\u5165\u91cf\uff1a1 UL\u3002<\/p>\n
GC\u6c7a\u5b9a
\n\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u4e2d\u306e\u30d4\u30ea\u30c0\u30d9\u30f3\u6b8b\u57fa\u306e\u304a\u304a\u3088\u305d\u306e\u6fc3\u5ea6\u306b\u3088\u308c\u3070\u3001\u30b5\u30f3\u30d7\u30eb\u6eb6\u6db2\u306e\u30d4\u30fc\u30af\u9762\u7a4d\u3068\u540c\u69d8\u306e\u30d4\u30fc\u30af\u9762\u7a4d\u3092\u6301\u3064\u6a19\u6e96\u4f5c\u696d\u6eb6\u6db2\u3092\u9078\u629e\u3057\u307e\u3059\u3002
\n\u4e0a\u8a18\u306eGC\u6761\u4ef6\u4e0b\u3067\u306f\u3001\u30d4\u30ea\u30c0\u30d9\u30f3\u306e\u4fdd\u6301\u6642\u9593\u306f\u7d0420\u30029\u5206\u3067\u3059\u3002<\/p>\n
GC-MS\u306e\u78ba\u8a8d
\nGC-MS\u64cd\u4f5c\u6761\u4ef6
\na\uff09\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u30a3\u30fc\u30ab\u30e9\u30e0\uff1a30 m x0\u300225mm\uff08i\u3002d\u3002\uff09
\n0\u300225um\u30d5\u30a3\u30eb\u30e0\u306e\u539a\u3055\u3001\u304a\u3088\u3073HP-5ms\u30b7\u30ea\u30ab\u6bdb\u7d30\u8840\u7ba1\u67f1\u307e\u305f\u306f\u540c\u7b49\u306e\u3082\u306e\u3002
\nb\uff09\u5217\u6e29\u5ea6\uff1a50\u2103\uff081\u5206\u4fdd\u7559\uff09\uff0810\u2103\/min\uff09 - 280\u2103\uff0810\u5206\uff09;
\nc\uff09\u6ce8\u5165\u30dd\u30fc\u30c8\u6e29\u5ea6\uff1a250 \u2103\uff1b
\nd\uff09\u30a4\u30f3\u30bf\u30fc\u30d5\u30a7\u30a4\u30b9\u6e29\u5ea6\uff1a280\u2103;
\ne\uff09\u96fb\u5b50\u30a4\u30aa\u30f3\u5316\u30e2\u30fc\u30c9\uff1aEL;
\nf\uff09\u30e9\u30a4\u30aa\u30f3\u5316\u30a8\u30cd\u30eb\u30ae\u30fc\uff1a70 eV\uff1a
\ng\uff09\u30ad\u30e3\u30ea\u30a2\u30ac\u30b9\uff1a\u30d8\u30ea\u30a6\u30e0\u3001\u7d14\u5ea6>99\u3002999\uff05\u3001\u6d41\u91cf1.0mL\/min:
\nh\uff09\u5674\u5c04\u30e2\u30fc\u30c9\uff1a\u5206\u5272\u3055\u308c\u3066\u30010\u5f8c\u306b\u30d0\u30eb\u30d6\u3092\u958b\u304d\u307e\u3059\u3002
\n75\u5206\uff1a
\ni\uff09\u6ce8\u5165\u91cf\uff1a1 UL\uff1a
\nj\uff09\u6c7a\u5b9a\u30e2\u30fc\u30c9\uff1aSIM\uff1a
\nk\uff09\u9078\u629e\u3055\u308c\u305f\u76e3\u8996\u30a4\u30aa\u30f3 (m\/z): 147\u3001309\u3001105\uff1a
\nl\uff09\u6eb6\u5a92\u4fdd\u8b77\u9045\u5ef6\uff1a5.0\u5206<\/p>\n
GC-MS\u306e\u78ba\u8a8d
\n\u4e0a\u8a18\u306e\u52d5\u4f5c\u6761\u4ef6\u306b\u5fdc\u3058\u3066\u3001\u30b5\u30f3\u30d7\u30eb\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\u3068\u6a19\u6e96\u4f5c\u696d\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\u306e\u4e21\u65b9\u3067\u540c\u3058\u4fdd\u6301\u6642\u9593\u306b\u30d4\u30fc\u30af\u304c\u8868\u793a\u3055\u308c\u308b\u5834\u5408\u3001\u6a19\u6e96\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\u3068\u30b5\u30f3\u30d7\u30eb\u30bd\u30ea\u30e5\u30fc\u30b7\u30e7\u30f3\u3092\u5206\u6790\u3057\u307e\u3059\u3002<\/p>\n
\u7a7a\u767d\u306e\u30c6\u30b9\u30c8
\n\u30d6\u30e9\u30f3\u30af\u30c6\u30b9\u30c8\u306f\u3001\u4e0a\u8a18\u306e\u624b\u9806\u306b\u5f93\u3063\u3066\u30b5\u30f3\u30d7\u30eb\u306e\u8ffd\u52a0\u306a\u3057\u3067\u5b9f\u65bd\u3055\u308c\u307e\u3059\u3002<\/p>\n
\u6c7a\u5b9a\u306e\u5236\u9650
\n\u6843\u3001\u68a8\u3001\u30a2\u30b9\u30d1\u30e9\u30ac\u30b9\u3001\u30b8\u30e3\u30ac\u30a4\u30e2\u3001\u30c8\u30a6\u30e2\u30ed\u30b3\u30b7\u3001\u305d\u3070\u3001\u8702\u871c\u3001\u9162\u3001\u30af\u30eb\u30df\u3001\u30eb\u30d3\u30c3\u30c8\u8089\u3001\u9d8f\u8089\u3001\u30a8\u30d3\u3001\u8336\u8449\u3001\u30bf\u30de\u30cd\u30ae\u3001\u9d8f\u30ec\u30d0\u30fc\u306e\u6e2c\u5b9a\u9650\u754c\u306f0.01mg\/kg\u3067\u3059\u3002<\/p>","protected":false},"excerpt":{"rendered":"
Principle The pyridaben residues were extracted with Ethyl acetate-Cyclohexane or Acetonitrile, purified by a gel permeation chromatography (GPC) or SPE, determinated by GC-ECD and confirmation by GC-MS. using external standard method. Reagents and materials All the reagents used should be analytically pure unless otherwise specified. “Water” is distilled water. 1. Ethyl acetate: HPLC grade. 2. Cyclohexane: HPLC grade. 3. Acetonitrile: HPLC grade 4. Hexane: HPLC grade. 5. Trichloromethane: HPLC grade. 6. Anhydrous sodium sulfate; Ignited at 650 c for 4 h and kept in a tightly closed container. 7. Sodium chloride. 8. Ethyl acetate + Cyclohexane (1+1, V\/V). 9. Hexane + Trichloromethane (9+1,V\/V). 10. Cyclohexane + Ethyl acetate (6+1, V\/V) […]<\/p>\n","protected":false},"author":1,"featured_media":3338,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[73],"tags":[],"class_list":["post-2802","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-food-and-drugs"],"acf":[],"_links":{"self":[{"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/posts\/2802","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/comments?post=2802"}],"version-history":[{"count":1,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/posts\/2802\/revisions"}],"predecessor-version":[{"id":4305,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/posts\/2802\/revisions\/4305"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/media\/3338"}],"wp:attachment":[{"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/media?parent=2802"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/categories?post=2802"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.pgeneral.com\/ja\/wp-json\/wp\/v2\/tags?post=2802"}],"curies":[{"name":"WP","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}