\u0645\u0628\u062f\u0623
\n\u062a\u0645 \u0627\u0633\u062a\u062e\u0631\u0627\u062c \u0628\u0642\u0627\u064a\u0627 \u0627\u0644\u0628\u064a\u0631\u064a\u062f\u064a\u0646 \u0645\u0639 \u0625\u064a\u062b\u064a\u0644 \u0623\u0633\u064a\u062a\u0627\u062a-\u0633\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646 \u0623\u0648 \u0627\u0644\u0623\u0633\u064a\u062a\u0648\u0646\u064a\u062a\u0631\u064a\u0644 \u060c \u0627\u0644\u062a\u064a \u062a\u0645 \u062a\u0646\u0642\u064a\u062a\u0647\u0627 \u0628\u0648\u0627\u0633\u0637\u0629 \u0643\u0631\u0648\u0645\u0627\u062a\u0648\u062c\u0631\u0627\u0641\u064a\u0627 \u062a\u063a\u0644\u063a\u0644 \u0647\u0644\u0627\u0645 (GPC) \u0623\u0648 SPE \u060c \u0648\u0627\u0644\u062a\u064a \u062a\u062d\u062f\u062f\u0647\u0627 GC-ECD \u0648\u062a\u0623\u0643\u064a\u062f GC-MS.<\/p>\n
\u0627\u0644\u0643\u0648\u0627\u0634\u0641 \u0648\u0627\u0644\u0645\u0648\u0627\u062f
\n\u064a\u062c\u0628 \u0623\u0646 \u062a\u0643\u0648\u0646 \u062c\u0645\u064a\u0639 \u0627\u0644\u0643\u0648\u0627\u0634\u0641 \u0627\u0644\u0645\u0633\u062a\u062e\u062f\u0645\u0629 \u0646\u0642\u064a\u0629 \u062a\u062d\u0644\u064a\u0644\u064a\u064b\u0627 \u0645\u0627 \u0644\u0645 \u064a\u0646\u0635 \u0639\u0644\u0649 \u062e\u0644\u0627\u0641 \u0630\u0644\u0643.
\n1. \u0625\u064a\u062b\u064a\u0644 \u0623\u0633\u064a\u062a\u0627\u062a: \u062f\u0631\u062c\u0629 HPLC.
\n2. Cyclohexane: HPLC Grade.
\n3. \u0623\u0633\u064a\u062a\u0648\u0646\u064a\u062a\u0631\u064a\u0644: \u062f\u0631\u062c\u0629 HPLC
\n4. \u0627\u0644\u0647\u0643\u0633\u0627\u0646: \u062f\u0631\u062c\u0629 HPLC.
\n5. Trichloromethane: HPLC \u062f\u0631\u062c\u0629.
\n6. \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645 \u0627\u0644\u0644\u0627\u0645\u0627\u0626\u064a\u0629.
\n4 \u0633\u0627\u0639\u0627\u062a \u0648\u0627\u0644\u0627\u062d\u062a\u0641\u0627\u0638 \u0628\u0647\u0627 \u0641\u064a \u062d\u0627\u0648\u064a\u0629 \u0645\u063a\u0644\u0642\u0629 \u0628\u0625\u062d\u0643\u0627\u0645.
\n7. \u0643\u0644\u0648\u0631\u064a\u062f \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645.
\n8. \u0625\u064a\u062b\u064a\u0644 \u0623\u0633\u064a\u062a\u0627\u062a + cyclohexane (1 + 1 \u060cV\/V).
\n9. Hexane + Trichloromethane (9 + 1 \u060c V\/V).
\n10. cyclohexane + ethyl acetate (6 + 1 \u060c V\/V)
\n11.
\n12. \u062d\u0644 \u0627\u0644\u0623\u0633\u0647\u0645 \u0627\u0644\u0642\u064a\u0627\u0633\u064a: \u0648\u0632\u0646 \u0628\u062f\u0642\u0629 \u0643\u0645\u064a\u0629 \u0645\u0639\u064a\u0646\u0629 \u0645\u0646 \u0645\u0639\u064a\u0627\u0631 \u0628\u064a\u0631\u064a\u062f\u0627 \u0648\u062a\u0648\u0635\u0644\u0647 \u0641\u064a \u062d\u062c\u0645 \u0635\u063a\u064a\u0631 \u0645\u0646 \u062e\u0644\u0627\u062a \u0627\u0644\u0625\u064a\u062b\u064a\u0644.
\n13. \u062d\u0644 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0642\u064a\u0627\u0633\u064a: \u062b\u0645 \u0642\u0645 \u0628\u062a\u062e\u0641\u064a\u0641 \u0645\u062d\u0644\u0648\u0644 \u0627\u0644\u0645\u062e\u0632\u0648\u0646 \u0627\u0644\u0642\u064a\u0627\u0633\u064a \u0628\u0627\u0633\u062a\u062e\u062f\u0627\u0645 \u062e\u0644\u0627\u062a \u0625\u064a\u062b\u064a\u0644 \u0625\u0644\u0649 \u0627\u0644\u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u0645\u0637\u0644\u0648\u0628 \u0643\u062d\u0644 \u0639\u0645\u0644 \u0642\u064a\u0627\u0633\u064a.
\n14. \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0643\u0631\u0628\u0648\u0646-PSA: 1 \u0645\u0644 \u060c 50 \u0645\u0644\u063a \u060c \u0646\u0634\u0637 \u0645\u0639 \u0623\u0633\u064a\u062a\u0648\u0646\u064a\u062a\u0631\u064a\u0644 3 \u0645\u0644 + \u0625\u064a\u062b\u064a\u0644 \u0623\u0633\u064a\u062a\u0627\u062a (10)
\n15. \u0623\u0646\u0627\u0628\u064a\u0628 HLB SPE: 3 \u0645\u0644 \u060c 60 \u0645\u0644\u063a \u060c \u0623\u0648 \u0645\u0627 \u064a\u0639\u0627\u062f\u0644\u0647\u0627.
\n(9) \u060c 2 \u0645\u0644 \u0645\u0646 \u062b\u0644\u0627\u062b\u064a \u0643\u0644\u0648\u0631\u0648 \u0645\u064a\u062b\u0627\u0646 \u0648 5 \u0645\u0644 \u0645\u0646 \u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0645\u0642\u0637\u0631 \u0642\u0628\u0644 \u0627\u0644\u0628\u062f\u0621.
\n16. \u0627\u0644\u0641\u064a\u0644\u0645: 0.45 \u0645\u064a\u0643\u0631\u0648\u0646.<\/p>\n
\u0627\u0644\u0623\u062c\u0647\u0632\u0629 \u0648\u0627\u0644\u0645\u0639\u062f\u0627\u062a
\n1. \u0643\u0631\u0648\u0645\u0627\u062a\u0648\u062c\u0631\u0627\u0641\u064a\u0627 \u0627\u0644\u063a\u0627\u0632: \u0645\u0632\u0648\u062f \u0628\u0640 ECD
\n2. \u0643\u0631\u0648\u0645\u0627\u062a\u0648\u062c\u0631\u0627\u0641\u064a\u0627 \u0627\u0644\u063a\u0627\u0632: \u0645\u062c\u0647\u0632 \u0628\u0637\u064a\u0627\u0641 \u0627\u0644\u0643\u062a\u0644\u0629 \u0627\u0644\u062a\u0623\u064a\u0646 \u0627\u0644\u0625\u0644\u0643\u062a\u0631\u0648\u0646.
\n3. \u0627\u0644\u062a\u0648\u0627\u0632\u0646 \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a: \u0634\u0639\u0648\u0631 0.01 \u062c\u0645.
\n4. \u0627\u0644\u062a\u0648\u0627\u0632\u0646 \u0627\u0644\u062a\u062d\u0644\u064a\u0644\u064a: \u0634\u0639\u0648\u0631 0.1 \u0645\u0644\u063a
\n5. \u0647\u0644\u0627\u0645 \u062c\u0644\u062f\u064a\u0648\u063a\u0631\u0627\u0641\u064a\u0627 \u0645\u0647\u0648\u0648\u0633 \u0628\u0645\u0636\u062e\u0629 isocratic \u0648\u062c\u0627\u0645\u0639 \u0627\u0644\u0643\u0633\u0631.
\n6. \u0623\u062c\u0647\u0632\u0629 \u0627\u0644\u0637\u0631\u062f \u0627\u0644\u0645\u0631\u0643\u0632\u064a: 4000 \u062f\u0648\u0631\u0629\/\u062f\u0642\u064a\u0642\u0629.
\n7. \u0645\u0628\u062e\u0631 \u0627\u0644\u0641\u0631\u0627\u063a \u0627\u0644\u062f\u0648\u0627\u0631
\n8. \u0639\u0645\u0648\u062f \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645 \u0627\u0644\u0644\u0627\u0645\u0627\u0626\u064a\u0629: 7.5 \u0633\u0645 \u00d7 1.5 \u0633\u0645 (\u0637. \u062f.
\n9. \u062e\u0644\u0627\u0637 \u062f\u0648\u0627\u0645\u0629.
\n10. \u0622\u0644\u0629 \u0627\u0644\u0645\u0648\u062c\u0627\u062a \u0641\u0648\u0642 \u0627\u0644\u0635\u0648\u062a\u064a\u0629.
\n11.
\n12. 50 \u0645\u0644 \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0637\u0631\u062f \u0627\u0644\u0645\u0631\u0643\u0632\u064a \u0627\u0644\u0628\u0644\u0627\u0633\u062a\u064a\u0643\u064a \u0627\u0644\u0633\u0648\u062f\u0627\u0621.<\/p>\n
\u0625\u0639\u062f\u0627\u062f \u0648\u062a\u062e\u0632\u064a\u0646 \u0639\u064a\u0646\u0629 \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631
\n\u062a\u062d\u0636\u064a\u0631 \u0639\u064a\u0646\u0629 \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631
\n1. \u0627\u0644\u062d\u0628\u0648\u0628 \u0648\u0627\u0644\u0634\u0627\u064a
\n\u0631\u0628\u0639 \u0627\u0644\u0639\u064a\u0646\u0629 \u0625\u0644\u0649 \u0643\u0627\u0644\u064a\u0641\u0648\u0631\u0646\u064a\u0627.
\n2. \u0627\u0644\u0641\u0648\u0627\u0643\u0647 \u0648\u0627\u0644\u062e\u0636\u0631\u0648\u0627\u062a
\n\u064a\u062a\u0645 \u062a\u0642\u0644\u064a\u0644 \u0627\u0644\u0639\u064a\u0646\u0629 \u0627\u0644\u0623\u0648\u0644\u064a\u0629 \u0627\u0644\u0645\u0634\u062a\u0631\u0643\u0629 \u0625\u0644\u0649 \u0643\u0627\u0644\u064a\u0641\u0648\u0631\u0646\u064a\u0627.<\/p>\n
3. \u0645\u0646\u062a\u062c\u0627\u062a \u0627\u0644\u0644\u062d\u0648\u0645 \u0648\u0627\u0644\u0644\u062d\u0648\u0645 \u060c \u0627\u0644\u0645\u0643\u0633\u0631\u0627\u062a
\n\u062e\u0630 \u0645\u0645\u062b\u0644 \u062d\u0648\u0627\u0644\u064a 1 \u0643\u062c\u0645 \u0645\u0646 \u0627\u0644\u0639\u064a\u0646\u0629.<\/p>\n
\u062a\u062e\u0632\u064a\u0646 \u0639\u064a\u0646\u0627\u062a \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631
\n\u064a\u062c\u0628 \u062a\u062e\u0632\u064a\u0646 \u0639\u064a\u0646\u0627\u062a \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631 \u0645\u0646 \u0627\u0644\u062d\u0628\u0648\u0628 \u0648\u0627\u0644\u0634\u0627\u064a \u0648\u0627\u0644\u0645\u0643\u0633\u0631\u0627\u062a \u0648\u0627\u0644\u062e\u0644 \u0648\u0627\u0644\u0639\u0633\u0644 \u0648\u0627\u0644\u0639\u0633\u0644 \u0628\u064a\u0646 0 \u2103 ~ 4 \u2103.<\/p>\n
\u0625\u062c\u0631\u0627\u0621
\n\u0627\u0650\u0633\u062a\u0650\u062e\u0644\u0627\u0635
\n1. \u0627\u0644\u062e\u0636\u0627\u0631 \u060c \u0627\u0644\u0641\u0648\u0627\u0643\u0647.
\n\u0648\u0632\u0646 10 \u063a\u0631\u0627\u0645\u0627\u062a (\u0628\u062f\u0642\u0629 0.01 \u063a\u0631\u0627\u0645) \u0645\u0646 \u0639\u064a\u0646\u0629 \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u064a \u0623\u0646\u0628\u0648\u0628 \u0637\u0631\u062f \u0645\u0631\u0643\u0632\u064a \u0628\u0644\u0627\u0633\u062a\u064a\u0643\u064a \u0645\u064f\u0633\u062f\u0651 \u0633\u0639\u0629 50 \u0645\u0644\u060c \u062b\u0645 \u0623\u0636\u0641 20 \u0645\u0644 \u0645\u0646 \u0623\u0633\u064a\u062a\u0627\u062a \u0627\u0644\u0625\u064a\u062b\u064a\u0644 + \u0633\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646 \u0645\u064f\u0633\u062a\u062e\u0644\u0635\u060c \u062b\u0645 \u0646\u0638\u0651\u0641\u0647 \u0628\u0633\u0631\u0639\u0629 100 \u0645\u064a\u0643\u0631\u0648\u0645\u062a\u0631\/\u062f\u0642\u064a\u0642\u0629 \u0644\u0645\u062f\u0629 \u062f\u0642\u064a\u0642\u0629 \u0648\u0627\u062d\u062f\u0629\u060c \u062b\u0645 \u0646\u0638\u0651\u0641\u0647 \u0628\u0633\u0631\u0639\u0629 4000 \u0645\u064a\u0643\u0631\u0648\u0645\u062a\u0631\/\u062f\u0642\u064a\u0642\u0629 \u0644\u0645\u062f\u0629 3 \u062f\u0642\u0627\u0626\u0642. \u0627\u0646\u0642\u0644 \u0627\u0644\u0633\u0627\u0626\u0644 \u0627\u0644\u0639\u0644\u0648\u064a \u0625\u0644\u0649 \u0623\u0646\u0628\u0648\u0628 \u0646\u0638\u064a\u0641 \u0622\u062e\u0631\u060c \u0648\u0643\u0631\u0651\u0631 \u0639\u0645\u0644\u064a\u0629 \u0627\u0644\u0627\u0633\u062a\u062e\u0644\u0627\u0635 \u0645\u0639 20 \u0645\u0644 \u0645\u0646 \u0623\u0633\u064a\u062a\u0627\u062a \u0627\u0644\u0625\u064a\u062b\u064a\u0644 + \u0633\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646 \u0645\u0631\u0629 \u0623\u062e\u0631\u0649. \u062a\u064f\u0645\u0631\u0651\u0631 \u0627\u0644\u0633\u0648\u0627\u0626\u0644 \u0627\u0644\u0639\u0644\u0648\u064a\u0629 \u0639\u0628\u0631 \u0639\u0645\u0648\u062f \u0645\u0646 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645 \u0627\u0644\u0644\u0627\u0645\u0627\u0626\u064a\u0629 \u0644\u0625\u0632\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u0621\u060c \u062b\u0645 \u062a\u064f\u062c\u0645\u0639 \u0627\u0644\u0646\u0641\u0627\u064a\u0627\u062a \u0627\u0644\u0633\u0627\u0626\u0644\u0629 \u0641\u064a \u0632\u062c\u0627\u062c\u0629 \u0645\u064f\u0631\u0643\u0651\u0632\u0629 \u0633\u0639\u0629 150 \u0645\u0644\u060c \u0648\u062a\u064f\u0643\u062b\u0651\u0641 \u062d\u062a\u0649 \u062a\u062c\u0641\u0651 \u062a\u0642\u0631\u064a\u0628\u064b\u0627 \u0628\u0648\u0627\u0633\u0637\u0629 \u0645\u064f\u0628\u062e\u0651\u0631 \u062f\u0648\u0627\u0631 \u0641\u064a \u062d\u0645\u0627\u0645 \u0645\u0627\u0626\u064a \u0628\u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 40 \u062f\u0631\u062c\u0629 \u0645\u0626\u0648\u064a\u0629. \u0623\u0630\u0628 \u0627\u0644\u0628\u0642\u0627\u064a\u0627 \u0645\u0639 10.0 \u0645\u0644 \u0645\u0646 \u0623\u0633\u064a\u062a\u0627\u062a \u0627\u0644\u0625\u064a\u062b\u064a\u0644 + \u0633\u064a\u0643\u0644\u0648\u0647\u0643\u0633\u0627\u0646\u060c \u062b\u0645\u0651 \u0631\u064f\u0634\u0651\u062d \u0639\u0628\u0631 \u0645\u064f\u0631\u0634\u0651\u062d \u063a\u0634\u0627\u0626\u064a \u0633\u0639\u0629 0.45 \u0645\u064a\u0643\u0631\u0648\u0645\u062a\u0631\u060c \u0648\u0627\u0646\u062a\u0638\u0631 \u062d\u062a\u0649 \u062a\u062a\u0645\u0651 \u062a\u0646\u0642\u064a\u062a\u0647\u0627.<\/p>\n
2. \u0627\u0644\u062c\u0648\u0632.
\n\u0627\u0644\u0648\u0632\u0646 10 (\u062f\u0642\u064a\u0642 \u0625\u0644\u0649 0. 01 \u062c\u0645) \u0645\u0646 \u0639\u064a\u0646\u0629 \u0627\u0644\u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u064a \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0637\u0631\u062f \u0627\u0644\u0645\u0631\u0643\u0632\u064a \u0627\u0644\u0628\u0644\u0627\u0633\u062a\u064a\u0643\u064a 50 \u0645\u0644.<\/p>\n
3. \u0627\u0644\u0634\u0627\u064a \u0648\u0627\u0644\u0628\u0635\u0644
\n\u0627\u0644\u0648\u0632\u0646 2. 5 \u063a\u0631\u0627\u0645 (\u062f\u0642\u064a\u0642 \u0625\u0644\u0649 0. 01 \u062c\u0645) \u0645\u0646 \u0627\u0644\u0639\u064a\u0646\u0627\u062a \u060c \u0641\u064a \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0637\u0631\u062f \u0627\u0644\u0645\u0631\u0643\u0632\u064a \u0627\u0644\u0628\u0644\u0627\u0633\u062a\u064a\u0643\u064a \u0627\u0644\u0633\u062a\u0639\u0633\u0651\u0646 50 \u0645\u0644 \u060c \u0623\u0636\u0641 15 \u0645\u0644 \u0645\u0646 \u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0645\u0642\u0637\u0631 \u060c \u0648\u0642\u0641 \u0644\u0645\u062f\u0629 1 \u0633\u0627\u0639\u0629.
\n\u064a\u062a\u0645 \u062a\u0645\u0631\u064a\u0631 \u0627\u0644\u0645\u0648\u0627\u062f \u0627\u0644\u0637\u0627\u0641\u064a\u0629 \u0645\u0646 \u062e\u0644\u0627\u0644 \u0639\u0645\u0648\u062f \u0645\u0646 \u0643\u0628\u0631\u064a\u062a\u0627\u062a \u0627\u0644\u0635\u0648\u062f\u064a\u0648\u0645 \u0627\u0644\u0644\u0627\u0645\u0627\u0626\u064a\u0629 \u0644\u0625\u0632\u0627\u0644\u0629 \u0627\u0644\u0645\u0627\u0621 \u060c \u0648\u062c\u0645\u0639 \u0627\u0644\u0646\u0641\u0627\u064a\u0627\u062a \u0627\u0644\u0633\u0627\u0626\u0644\u0629 \u0625\u0644\u0649 \u0632\u062c\u0627\u062c\u0629 \u0645\u0631\u0643\u0632\u0629 150 \u0645\u0644 \u0648\u062a\u0643\u062b\u064a\u0641 \u062d\u062a\u0649 \u062a\u062c\u0641 \u062a\u0642\u0631\u064a\u0628\u064b\u0627 \u0628\u0648\u0627\u0633\u0637\u0629 \u0645\u0628\u062e\u0631 \u062f\u0648\u0627\u0631 \u0645\u0639 \u062d\u0645\u0627\u0645 \u0645\u0627\u0626\u064a 40 \u2103.<\/p>\n
\u0627\u0644\u062a\u0646\u0638\u064a\u0641
\n\u062a\u0646\u0638\u064a\u0641 GPC \u0644\u0644\u0641\u0648\u0627\u0643\u0647 \u0627\u0644\u062e\u0636\u0627\u0631 \u0648\u0627\u0644\u062d\u0628\u0648\u0628 \u0648\u0627\u0644\u062c\u0648\u0632 \u0648\u0627\u0644\u0643\u0628\u062f \u0627\u0644\u062f\u062c\u0627\u062c.
\n1. \u062d\u0627\u0644\u0629 \u062a\u0634\u063a\u064a\u0644 GPC
\n\u0623) \u0639\u0645\u0648\u062f GPC: 300 \u0645\u0645 10 \u0645\u0645 (\u0637. \u062f.) \u060c Bio Beads S-X3 \u0623\u0648 \u0645\u0627 \u064a\u0639\u0627\u062f\u0644\u0647\u0627:
\n\u0628) \u0627\u0644\u0645\u0631\u062d\u0644\u0629 \u0627\u0644\u0645\u062a\u0646\u0642\u0644\u0629: \u0623\u0633\u064a\u062a\u0627\u062a \u0633\u064a\u0643\u0644\u0648\u0647\u064a\u0643\u0633\u0627\u0646 \u0625\u064a\u062b\u064a\u0644 (1+1):
\n\u062c) \u0645\u0639\u062f\u0644 \u0627\u0644\u062a\u062f\u0641\u0642: 4.7 \u0645\u0644\/\u062f\u0642\u064a\u0642\u0629:
\n\u062f) \u062d\u062c\u0645 \u0627\u0644\u062d\u0642\u0646 \u0641\u064a \u062d\u0644\u0642\u0629 \u0627\u0644\u0639\u064a\u0646\u0629: 5 \u0645\u0644:
\n\u0647\u0640) \u0648\u0642\u062a \u062c\u0645\u0639 \u0627\u0644\u0646\u062e\u0628\u0629: 7.5 \u062f\u0642\u064a\u0642\u0629 ~ 12.<\/p>\n
2. \u062e\u0637\u0648\u0629 \u062a\u0646\u0638\u064a\u0641 GPC<\/p>\n
\u0646\u0642\u0644 \u0627\u0644\u062d\u0644 \u0627\u0644\u0630\u064a \u062a\u0645 \u0627\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u064a\u0647 \u0645\u0646 \u0642\u0628\u0644 \u0625\u0644\u0649 \u0639\u0645\u0648\u062f GPC \u0645\u0639 \u0627\u0644\u0645\u0639\u0644\u0645\u0627\u062a \u0627\u0644\u0645\u0648\u0636\u062d\u0629 \u0641\u064a \u0627\u0644\u062e\u0637\u0648\u0629 \u0627\u0644\u0623\u0648\u0644\u0649.
\n\u064a\u062a\u0645 \u062c\u0645\u0639 \u0627\u0644\u0634\u0637\u0641 \u0641\u064a \u0623\u0646\u0628\u0648\u0628 \u0646\u0638\u064a\u0641 \u0648\u062a\u0628\u062e\u0631 \u0625\u0644\u0649 \u0627\u0644\u062c\u0641\u0627\u0641 \u0639\u0646\u062f 35 \u2103 \u062a\u062d\u062a \u062a\u064a\u0627\u0631 \u0645\u0646 \u0627\u0644\u0646\u064a\u062a\u0631\u0648\u062c\u064a\u0646 \u0648\u0625\u0639\u0627\u062f\u0629 \u062a\u062f\u0648\u064a\u0631\u0647 \u0641\u064a \u062e\u0644\u0627\u062a \u0625\u064a\u062b\u064a\u0644 1.0 \u0645\u0644 \u0644\u062a\u062d\u062f\u064a\u062f\u0647 \u0648\u0627\u0644\u062a\u0634\u0643\u0644.<\/p>\n
3. \u062a\u0646\u0638\u064a\u0641 SPE \u0644\u0644\u062e\u0644 \u0648\u0627\u0644\u0639\u0633\u0644
\n\u0627\u0644\u0648\u0632\u0646 2.5 \u063a\u0631\u0627\u0645 \u0645\u0646 \u0627\u0644\u0639\u064a\u0646\u0627\u062a \u0641\u064a \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0637\u0631\u062f \u0627\u0644\u0645\u0631\u0643\u0632\u064a \u0627\u0644\u0628\u0644\u0627\u0633\u062a\u064a\u0643\u064a \u060c \u0623\u0636\u0641 5 \u0645\u0644 \u0645\u0646 \u0627\u0644\u0645\u0627\u0621 \u0627\u0644\u0645\u0642\u0637\u0631 \u0648\u0627\u0644\u062f\u0648\u0627\u0645\u0629 \u0644\u0645\u062f\u0629 30 \u062b\u0627\u0646\u064a\u0629.<\/p>\n
4. \u062a\u0646\u0638\u064a\u0641 SPE \u0644\u0644\u0634\u0627\u064a \u0648\u0627\u0644\u0628\u0635\u0644
\n\u0646\u0642\u0644 \u0627\u0644\u0645\u062d\u0644\u0648\u0644 \u0627\u0644\u0630\u064a \u062a\u0645 \u0627\u0644\u062d\u0635\u0648\u0644 \u0639\u0644\u064a\u0647 \u0642\u0628\u0644 \u0623\u0646\u0628\u0648\u0628 \u0627\u0644\u0643\u0631\u0628\u0648\u0646 PSA \u060c \u0634\u0637\u0641 \u0645\u0639 1. 5 \u0645\u0644 \u0645\u0646 \u0623\u0633\u064a\u062a\u0627\u062a \u0633\u064a\u0643\u0644\u0648\u0647\u064a\u0643\u0633\u0627\u0646 + \u0625\u064a\u062b\u064a\u0644 \u0625\u064a\u062b\u064a\u0644.<\/p>\n
\u062a\u062d\u062f\u064a\u062f GC
\n\u0634\u0631\u0648\u0637 \u062a\u0634\u063a\u064a\u0644 GC
\n\u0623) \u0627\u0644\u0639\u0645\u0648\u062f: DB-1301 30 \u0645 0. 25 \u0645\u0645 (i.d.) x 0. 25 um \u0623\u0648 \u0645\u0627 \u064a\u0639\u0627\u062f\u0644\u0647\u0627 \u061b
\n\u0628) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u0639\u0645\u0648\u062f: 50 \u2103 (20 \u2103\/min) - 200 \u2103 (5 \u2103\/min) - 260 \u2103 (10min).
\n\u062c) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0645\u0646\u0641\u0630 \u0627\u0644\u062d\u0642\u0646: 260 \u062c:
\n\u062f) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 ECD: 300 \u062c:
\n\u0647) \u063a\u0627\u0632 \u0627\u0644\u0646\u0627\u0642\u0644: \u0627\u0644\u0646\u064a\u062a\u0631\u0648\u062c\u064a\u0646 (\u0646\u0642\u0627\u0621> 99.999 \u066a \u0645\u0639\u062f\u0644 \u0627\u0644\u062a\u062f\u0641\u0642: 2 \u0645\u0644 {{url_placeholder_0}}) \u061b
\n\u0648) \u0648\u0636\u0639 \u0627\u0644\u062d\u0642\u0646: \u0627\u0646\u0642\u0633\u0627\u0645.
\n\u0632) \u062d\u062c\u0645 \u0627\u0644\u062d\u0642\u0646: 1 ul.<\/p>\n
\u062a\u062d\u062f\u064a\u062f GC
\n\u0648\u0641\u0642\u064b\u0627 \u0644\u0644\u062a\u0631\u0643\u064a\u0632 \u0627\u0644\u062a\u0642\u0631\u064a\u0628\u064a \u0644\u0645\u062e\u0644\u0641\u0627\u062a Pyridaben \u0641\u064a \u0645\u062d\u0644\u0648\u0644 \u0627\u0644\u0639\u064a\u0646\u0629 \u060c \u062d\u062f\u062f \u062d\u0644 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0642\u064a\u0627\u0633\u064a \u0645\u0639 \u0645\u0633\u0627\u062d\u0629 \u0630\u0631\u0648\u0629 \u0645\u0645\u0627\u062b\u0644\u0629 \u0644\u0645\u062d\u0644\u0648\u0644 \u0627\u0644\u0639\u064a\u0646\u0629.
\n\u0641\u064a \u0638\u0644 \u0638\u0631\u0648\u0641 GC \u0627\u0644\u0645\u0630\u0643\u0648\u0631\u0629 \u0623\u0639\u0644\u0627\u0647 \u060c \u064a\u0628\u0644\u063a \u0648\u0642\u062a \u0627\u0644\u0627\u062d\u062a\u0641\u0627\u0638 \u0628\u064a\u0631\u064a\u062f\u064a\u0646 \u062d\u0648\u0627\u0644\u064a 20 \u062f\u0642\u064a\u0642\u0629.<\/p>\n
\u062a\u0623\u0643\u064a\u062f GC-MS
\n\u0634\u0631\u0648\u0637 \u062a\u0634\u063a\u064a\u0644 GC-MS
\n\u0623) \u0627\u0644\u0639\u0645\u0648\u062f \u0627\u0644\u0643\u0631\u0648\u0645\u0627\u062a\u0648\u063a\u0631\u0627\u0641\u064a: 30 \u0645 \u00d7 0. 25 \u0645\u0645 (\u0637. \u062f.)
\n0. 25 \u0633\u0645 \u0633\u0645\u0643 \u0627\u0644\u0641\u064a\u0644\u0645 \u060c \u0648\u0639\u0645\u0648\u062f HP-5Ms Silica \u0627\u0644\u0634\u0639\u064a\u0631\u0627\u062a \u0627\u0644\u062f\u0645\u0648\u064a\u0629 \u0623\u0648 \u0645\u0627 \u064a\u0639\u0627\u062f\u0644\u0647\u0627 \u061b
\n\u0628) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u0639\u0645\u0648\u062f: 50 \u2103 (\u0639\u0642\u062f 1 \u062f\u0642\u064a\u0642\u0629) (10 \u2103\/min) - 280 \u2103 (10min) \u061b
\n\u062c) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0645\u0646\u0641\u0630 \u0627\u0644\u062d\u0642\u0646: 250 \u2103\uff1b
\n\u062f) \u062f\u0631\u062c\u0629 \u062d\u0631\u0627\u0631\u0629 \u0627\u0644\u0648\u0627\u062c\u0647\u0629: 280 \u2103 \u061b
\n\u0647) \u0648\u0636\u0639 \u0627\u0644\u062a\u0623\u064a\u0646 \u0627\u0644\u0625\u0644\u0643\u062a\u0631\u0648\u0646: EL \u061b
\n\u0648) \u0637\u0627\u0642\u0629 \u0627\u0644\u0623\u0633\u062f: 70 \u0641\u0648\u0644\u062a:
\n\u0632) \u0627\u0644\u063a\u0627\u0632 \u0627\u0644\u0646\u0627\u0642\u0644: \u0627\u0644\u0647\u064a\u0644\u064a\u0648\u0645\u060c \u0646\u0642\u0627\u0621 > 99.999%\u060c \u0645\u0639\u062f\u0644 \u0627\u0644\u062a\u062f\u0641\u0642 1.0 \u0645\u0644\/\u062f\u0642\u064a\u0642\u0629:
\n\u062d) \u0648\u0636\u0639 \u0627\u0644\u062d\u0642\u0646: \u0627\u0646\u0642\u0633\u0627\u0645 \u060c \u0627\u0641\u062a\u062d \u0627\u0644\u0635\u0645\u0627\u0645 \u0628\u0639\u062f 0.
\n75 \u062f\u0642\u064a\u0642\u0629:
\n\u0637) \u062d\u062c\u0645 \u0627\u0644\u062d\u0642\u0646: 1 ul:
\n\u064a) \u0648\u0636\u0639 \u0627\u0644\u062a\u062d\u062f\u064a\u062f: SIM:
\n\u0643) \u0623\u064a\u0648\u0646\u0627\u062a \u0627\u0644\u0645\u0631\u0627\u0642\u0628\u0629 \u0627\u0644\u0645\u062e\u062a\u0627\u0631\u0629 (\u0645\/\u0632): 147\u060c 309\u060c 105:
\n\u0644) \u062a\u0623\u062e\u064a\u0631 \u062d\u0645\u0627\u064a\u0629 \u0627\u0644\u0645\u0630\u064a\u0628\u0627\u062a: 5.0 \u062f\u0642\u064a\u0642\u0629.<\/p>\n
\u062a\u0623\u0643\u064a\u062f GC-MS
\n\u0648\u0641\u0642\u064b\u0627 \u0644\u062d\u0627\u0644\u0629 \u0627\u0644\u062a\u0634\u063a\u064a\u0644 \u0623\u0639\u0644\u0627\u0647 \u060c \u0642\u0645 \u0628\u062a\u062d\u0644\u064a\u0644 \u0627\u0644\u062d\u0644 \u0627\u0644\u0642\u064a\u0627\u0633\u064a \u0648\u062d\u0644 \u0627\u0644\u0639\u064a\u0646\u0629 \u060c \u0625\u0630\u0627 \u0638\u0647\u0631\u062a \u0630\u0631\u0648\u0629 \u0641\u064a \u0646\u0641\u0633 \u0648\u0642\u062a \u0627\u0644\u0627\u0633\u062a\u0628\u0642\u0627\u0621 \u0644\u0643\u0644 \u0645\u0646 \u062d\u0644 \u0627\u0644\u0639\u064a\u0646\u0629 \u0648\u062d\u0644 \u0627\u0644\u0639\u0645\u0644 \u0627\u0644\u0642\u064a\u0627\u0633\u064a.<\/p>\n
\u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u0627\u0631\u063a
\n\u0633\u064a\u062a\u0645 \u0625\u062c\u0631\u0627\u0621 \u0627\u062e\u062a\u0628\u0627\u0631 \u0641\u0627\u0631\u063a \u0648\u0641\u0642\u064b\u0627 \u0644\u0644\u0625\u062c\u0631\u0627\u0621\u0627\u062a \u0627\u0644\u0645\u0630\u0643\u0648\u0631\u0629 \u0623\u0639\u0644\u0627\u0647 \u062f\u0648\u0646 \u0625\u0636\u0627\u0641\u0629 \u0639\u064a\u0646\u0629.<\/p>\n
\u0627\u0644\u062d\u062f \u0645\u0646 \u0627\u0644\u0642\u0631\u0627\u0631
\n\u062d\u062f\u0648\u062f \u0627\u0644\u062a\u062d\u062f\u064a\u062f \u0641\u064a \u0627\u0644\u062e\u0648\u062e \u0648\u0627\u0644\u0643\u0645\u062b\u0631\u0649 \u0648\u0627\u0644\u0647\u0644\u064a\u0648\u0646 \u0648\u0627\u0644\u0628\u0637\u0627\u0637\u0633 \u0648\u0627\u0644\u0630\u0631\u0629 \u0648\u0627\u0644\u062d\u0646\u0637\u0629 \u0627\u0644\u0633\u0648\u062f\u0627\u0621 \u0648\u0627\u0644\u0639\u0633\u0644 \u0648\u0627\u0644\u062e\u0644 \u0648\u0627\u0644\u062c\u0648\u0632 \u0648\u0644\u062d\u0645 \u0627\u0644\u0631\u0648\u0628\u064a\u062a \u0648\u0644\u062d\u0645 \u0627\u0644\u062f\u062c\u0627\u062c \u0648\u0627\u0644\u0631\u0648\u0628\u064a\u0627\u0646 \u0648\u0623\u0648\u0631\u0627\u0642 \u0627\u0644\u0634\u0627\u064a \u0648\u0627\u0644\u0628\u0635\u0644 \u0648\u0643\u0628\u062f \u0627\u0644\u062f\u062c\u0627\u062c \u0647\u064a 0.01 \u0645\u0644\u063a\u0645 \/ \u0643\u063a\u0645.<\/p>","protected":false},"excerpt":{"rendered":"
Principle The pyridaben residues were extracted with Ethyl acetate-Cyclohexane or Acetonitrile, purified by a gel permeation chromatography (GPC) or SPE, determinated by GC-ECD and confirmation by GC-MS. using external standard method. Reagents and materials All the reagents used should be analytically pure unless otherwise specified. “Water” is distilled water. 1. Ethyl acetate: HPLC grade. 2. […]<\/p>\n","protected":false},"author":1,"featured_media":3338,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[73],"tags":[],"class_list":["post-2802","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-food-and-drugs"],"acf":[],"_links":{"self":[{"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/posts\/2802","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/comments?post=2802"}],"version-history":[{"count":1,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/posts\/2802\/revisions"}],"predecessor-version":[{"id":4305,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/posts\/2802\/revisions\/4305"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/media\/3338"}],"wp:attachment":[{"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/media?parent=2802"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/categories?post=2802"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.pgeneral.com\/ar\/wp-json\/wp\/v2\/tags?post=2802"}],"curies":[{"name":"WP","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}